Synthesis, structural characterization and determination of the nitro-containing explosives detection potential of supramolecular lanthanum complex and Lanthana nanoparticles
Yazarlar (8)
Doç. Dr. Füreya Elif ÖZTÜRKKAN
Kafkas Üniversitesi, Türkiye
Elaheh Teymouri
University Of Tabriz, İran
Mustafa Yüksek
Iskenderun Technical University, Türkiye
Elif Akhüseyin Yıldız
Ankara Üniversitesi, Türkiye
Doç. Dr. Mustafa SERTÇELİK
Kafkas Üniversitesi, Türkiye
Abdolali Alemi
University Of Tabriz, İran
Prof. Dr. Hacali NECEFOĞLU
Kafkas Üniversitesi, Türkiye
Tuncer Hökelek
Hacettepe Üniversitesi, Türkiye
| Makale Türü |
Özgün Makale
(SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
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| Dergi Adı | Materials Science and Engineering B (Q2) | ||
| Dergi ISSN | 0921-5107 Wos Dergi Scopus Dergi | ||
| Dergi Tarandığı Indeksler | SCI-Expanded | ||
| Makale Dili | Türkçe | Basım Tarihi | 04-2023 |
| Cilt / Sayı / Sayfa | 290 / 1 / – | DOI | 10.1016/j.mseb.2023.116331 |
| Makale Linki | https://doi.org/10.1016/j.mseb.2023.116331 | ||
| Özet |
| A novel nanoparticle sized complex, [La(HO-C6H4-CH2COO)3(H2O)].(H2O), has been prepared by the reaction of LaIII ion and a versatile carboxylate ligand, 4-hydroxyphenylacetatic acid. The obtained complex was structurally characterized by using single crystal X-ray diffraction, SEM-EDS and FT-IR spectroscopy. Then, we synthesized La2O3 nanoparticles by the calcination of the complex and characterized its features by powder X-ray diffraction and SEM analysis. Average particle sizes of the complex and La2O3 particles were determined 19.6 nm and 44.02 nm, respectively. The bulk form of La2O3 (bulk) was bought commercially. The linear optical absorption traces of all materials were recorded by using UV–Vis spectrophotometer. The nitro-containing explosive detection potentials of complex, nanoparticles and bulk materials were investigated by using fluorescence spectrophotometer which is measured the fluorescence quenching of these three materials in nitro-containing media. It was found that all of the studied materials are good candidates especially for the detection of nitroaromatic compounds. |
| Anahtar Kelimeler |
| Lanthanum complex | 4-hydroxyphenylacetic acid | XRD | Fluorescence | Nitro-containing media |
Science Direct
Synthesis, structural characterization and determination of the nitro-containing explosives detection potential of supramolecular lanthanum complex and Lanthana nanoparticles
BM Sürdürülebilir Kalkınma Amaçları
| Atıf Sayıları | |
| WoS | 2 |
| SCOPUS | 3 |
| Google Scholar | 3 |