bis nicotinamide and bis N N diethyl nicotinamide p hydroxybenzoate complexes of Ni II Cu II and Zn II Spectrothermal studies
Yazarlar (4)
H. Icbudak Ondokuz Mayis Üniversitesi, Türkiye
Z. Heren Ondokuz Mayis Üniversitesi, Türkiye
D. Ali Kose Kafkas Üniversitesi, Türkiye
Prof. Dr. Hacali NECEFOĞLU Kafkas Üniversitesi, Türkiye
| Makale Türü |
Özgün Makale
(SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
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| Dergi Adı | Journal of Thermal Analysis and Calorimetry | ||
| Dergi ISSN | 1388-6150 Wos Dergi Scopus Dergi | ||
| Dergi Tarandığı Indeksler | SCI-Expanded | ||
| Makale Dili | İngilizce | Basım Tarihi | 01-2004 |
| Kabul Tarihi | – | Yayınlanma Tarihi | 01-06-2004 |
| Cilt / Sayı / Sayfa | 76 / 3 / 837–851 | DOI | 10.1023/B:JTAN.0000032269.12381.42 |
| Makale Linki | https://link.springer.com/10.1023/B:JTAN.0000032269.12381.42 | ||
| Özet |
| The mixed-ligand p-hydroxybenzoate complexes of Ni(II), Cu(II) and Zn(II) with nicotinamide and N,N-diethylnicotinamide were synthesized and characterized by elemental analysis, magnetic susceptibility measurements and mass spectrometry. The thermal behavior of the complexes was studied by simultaneous TG, DTG and DTA methods in static air atmosphere. The infrared spectral characteristics of the complexes are also discussed. The complexes contain two water molecules, two p-hydroxybenzoato (p-hba) and two nicotinamide (na) (or diethylnicotinamide (dena)) ligands per formula unit. In these complexes, all ligands are coordinated to the metal ion as monodendate ligands. In Zn(II)-na and Cu(II)-dena complexes, thep-hydroxybenzoate behaves as bidentate chelating ligand through carboxylic oxygen atoms. The decomposition pathways and the stability of the complexes are interpreted in the terms of … |
| Anahtar Kelimeler |
| Diethylnicotinamide | Metal complexes | Nicotinamide | p-hydroxybenzoato | Thermal decomposition |
BM Sürdürülebilir Kalkınma Amaçları
| Atıf Sayıları | |
| Google Scholar | 53 |
| Web of Science | 34 |
| Scopus | 36 |